Scanning Electron Microscope (SEM)
Installed in 2008, our JEOL 6490LV SEM has an SE, BSE, and an EDAX Genesis EDS detector. The SEM can operate in high- or low-vacuum modes. Only BSE and X-ray (EDS) signals can be detected in low-vacuum mode. The BSE detector can be used in composition, topographic, or shadow modes (by subtracting or adding signals from the different BSE diodes). Topographic and shadow modes are similar to SE images. In high-vacuum mode, BSE and SE images can be displayed simultaneously or mixed. Magnifications from approximately 50x to 300,000x are achievable in secondary electron (SE) or backscattered electron imaging mode. The EDS detector can be used to create qualitative and semi-quantitative elemental analysis of materials, X-ray maps, and X-ray line-scans.
Requirements of Samples
- Because the SEM can operate in high- or low-vacuum modes, a conductive coating is not required for insulating samples. However, conductive samples (or those with a conductive coating) are preferable for optimal image acquisition and chemical analysis. Carbon coating is available in the DGS Electron Microbeam Laboratory. Contact James Maner for details.
- Samples must be dry (water is the main concern, but some oil-saturated samples might also be unsuitable, for example).
Sample Shape and Size
- Typical samples are thin sections and materials < 1-cm diameter.
- Four 1-cm diameter samples can be loaded into the SEM simultaneously.
- Somewhat larger samples, up to a 5 cm in diameter, can also be used. Users must contact James Maner before using the SEM to examine large samples approaching 5 cm or larger. Large samples pose the possibility of colliding with the detectors.
- The stage can be tilted up to 55° from horizontal.
Requesting instrument time
All users should fill out the ‘Request to use the EPMA,ESEM,SEM‘ form. The purpose of the form is to communicate the goals of the project to the lab manager and lab assistant. The form also serves as an agreement between the user, advisor/account holder (if applicable), and the lab manager. Any questions regarding the form should be directed to the lab manager.
Internal (UT-Austin): $150/shift
Scheduling Time on the SEM
Anyone interested in using the SEM should fill out the form above. James Maner will contact you to discuss your analytical goals, sample preparation, and scheduling. Once your request for instrument time is approved, use the “Scheduling and Rate Structure” tab on the right hand side of the page for information on scheduling instrument time.